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PDF Editor FAQ

What happens when 2,4-Dinitrophenylhydrazine reacts with acetone in the presence of an acid?

The reaction of 2,4-dinitrophenylhydrazine (2,4-DNPH) and acetone in the presence of acid leads to the formation of acetone 2,4-dinitrophenylhydrazone as shown in the equation below.This use to be an important reaction that was used for the identification of unknown aldehydes and ketones. In this process the unknown was treated with 2,4-DNPH and the hydrazone isolated and recrystallized. After drying, a melting point was taken. There are vast tables of the melting points of 2,4-DNPHs so you’d find the one with the same melting point. If there were two that were the same or, at least very close, you’d make a second derivative and go through the same exercise. The chances of two derivatives having the the same melting point for one aldehyde/ketone as for another are very slim. Still, you could make a third…

What is Recrystallization temperature?

Recrystallization temperature is a particular temperature point below the melting point of a metal (or material). Usually, metals, in microscopic scale are made up of grain like particles. At recrystallization temperature, if you impart enough force, you can easily succeed to change the size and shape of these grains and this might make the metal more ductile and more stress-relieved. This is because the grains at this temperature, make the metal behave in plastic manner, allowing them to deform greatly for very less force application.Forging(all except a few processes like cold rolling) is the set of manufacturing processes that extensively makes use of this temperature, which is the property of a metal, to deform it and produce suitable product out of it.

Can crystalline solids be converted into amorphous solids?

Yes they can.But not very easily, it can be converted by many method but still involves various tedious steps.As far as I know,The simplest method is to convert it by heating it till its melting point and then quickly cool it down rapidly (With liquid N2). This will prevent recrystallization, Any future heating past its crystallization temperature will of course lead to recrystallization.

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